C₁₃H₁₈BrNO₄S

Base Information

Chemical Name:C₁₃H₁₈BrNO₄S
CAS No.:947321-04-2
Molecular Formula:C₁₃H₁₈BrNO₄S
Molecular Weight:364.26
Hs Code.:

C<sub>13</sub>H<sub>18</sub>BrNO<sub>4</sub>S

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Suppliers and Price of C₁₃H₁₈BrNO₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₈BrNO₄S

Chemical Property:

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Technology Process of C₁₃H₁₈BrNO₄S

There total 15 articles about C₁₃H₁₈BrNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₂BrNO₄S

: 947321-04-2
C₁₃H₁₈BrNO₄S

Guidance literature:: With hydrogenchloride; water; In methanol; at 25 ℃;
DOI:10.1016/j.bmcl.2011.02.038

Reference yield:

: C₂₁H₃₀BrNO₆S

: 947321-04-2
C₁₃H₁₈BrNO₄S

Guidance literature:: Multi-step reaction with 3 steps

1: ChiralPak-AD / tetrahydrofuran; hexane; tert-butyl methyl ether

2: hydrogenchloride / 1,4-dioxane / 25 °C

3: hydrogenchloride; water / methanol / 25 °C

With hydrogenchloride; water; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; tert-butyl methyl ether;
DOI:10.1016/j.bmcl.2011.02.038

Reference yield:

: C₁₄H₁₆BrNO₅S

: 947321-04-2
C₁₃H₁₈BrNO₄S

Guidance literature:: Multi-step reaction with 8 steps

1: dmap; triethylamine / 50 °C

2: methanol; caesium carbonate / 25 °C

3: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide / 25 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / -70 °C

5: toluene-4-sulfonic acid / dichloromethane / Reflux

6: ChiralPak-AD / tetrahydrofuran; hexane; tert-butyl methyl ether

7: hydrogenchloride / 1,4-dioxane / 25 °C

8: hydrogenchloride; water / methanol / 25 °C

With hydrogenchloride; methanol; dmap; lithium aluminium tetrahydride; water; sulfur trioxide pyridine complex; caesium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; tert-butyl methyl ether; dimethyl sulfoxide; 3: Parikh-Doering oxidation;
DOI:10.1016/j.bmcl.2011.02.038