cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}

Base Information

Chemical Name:cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}
CAS No.:123239-10-1
Molecular Formula:C₃₄H₃₄MoN₂O₆P₂
Molecular Weight:724.541
Hs Code.:

cis-Mo(CO)4{Ph<sub>2</sub>PNH(CH<sub>2</sub>)2O(CH<sub>2</sub>)2O(CH<sub>2</sub>)2NHPPh<sub>2</sub>}

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Chemical Property of cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}

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Technology Process of cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}

There total 1 articles about cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 12146-37-1,124717-04-0
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum⁽⁰⁾

: 123207-83-0
(C₆H₅)2PNHCH₂(CH₂OCH₂)2CH₂NHP(C₆H₅)2

: 123239-10-1
cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}

Guidance literature:: In dichloromethane; high-dilution conditions, N2-atmosphere; adding simultaneously two educts to CH2Cl2 during 15-20h (shielding from light); stirring 72h at 20°C; concentrating (rotary evaporator); adding cellulose powder; concentrating (rotary evaporator); adding cellulose powder; purification over a column (hexane/CH2Cl2 and CH2Cl2); elemental analysis;

Reference yield: 8.0%

: 123239-10-1
cis-Mo(CO)4{Ph₂PNH(CH₂)2O(CH₂)2O(CH₂)2NHPPh₂}

: 917-54-4
methyllithium

: 123239-17-8
fac-Mo(CO)3(MeCOAl)(Ph₂PN(CH₂)2O(CH₂)2O(CH₂)2NPPh₂)

Guidance literature:: With aluminum tri-bromide; In tetrahydrofuran; diethyl ether; N2-atmosphere; to Mo-complex in THF addn. of MeLi in Et2O; after 5 min addn. of AlBr3 to Mo-complex; solution allowed to stand for 5h; washing orange powder with THF; elemental analysis;