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Technology Process of (14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate

(14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate

Base Information
  • Chemical Name:(14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate
  • CAS No.:88635-33-0
  • Molecular Formula:C36H40N6Ni*2F6P
  • Molecular Weight:905.372
  • Hs Code.:
(14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9<sup>(28)</sup>,12,14,19,21,26-nonaene-k<sup>(4)</sup>N)nickel(II) hexafluorophosphate

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Chemical Property of (14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate
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Technology Process of (14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate

There total 1 articles about (14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

{Ni(Ph<sub>2</sub>(MeO)2{16}cylidene)}(PF<sub>6</sub>)

{Ni(Ph2(MeO)2{16}cylidene)}(PF6)

N,N′-dimethyl-m-xylylenediamine
23399-62-4

N,N′-dimethyl-m-xylylenediamine

(14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9<sup>(28)</sup>,12,14,19,21,26-nonaene-k<sup>(4)</sup>N)nickel(II) hexafluorophosphate
88635-33-0

(14,20-dimethyl-2,12-diphenyl-3,11,15,19,22,26-hexaazatricyclo[11.7.7.1(5,9)]octacosa-1,5,7,9(28),12,14,19,21,26-nonaene-k(4)N)nickel(II) hexafluorophosphate

Guidance literature:
In acetonitrile; equimolar amt. of Ni-complex in CH3CN and C6H4(CH2NMe2)2 in CH3CN was very slowly dripped into stirred refluxing CH3CN for ca. 2 h; rotavaporated, chromd. on neutral alumina with CH3CN as eluent, evapd. to dryness, recrystd. from CH3CN-EtOH; elem. anal.;
upstream raw materials:

N,N′-dimethyl-m-xylylenediamine

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