diphenyltridec-2-enylphosphine borane

Base Information

Chemical Name:diphenyltridec-2-enylphosphine borane
CAS No.:920276-29-5
Molecular Formula:C₂₅H₃₈BP
Molecular Weight:380.361
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyltridec-2-enylphosphine borane

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Technology Process of diphenyltridec-2-enylphosphine borane

There total 1 articles about diphenyltridec-2-enylphosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 127686-75-3
allyl(diphenyl)phosphine-borane

: 112-41-4,25067-08-7,62132-67-6
1-dodecene

: 920276-29-5,920017-04-5
diphenyltridec-2-enylphosphine borane

Guidance literature:: In dichloromethane; (Ar); soln. of P-B compd. (1 equiv.) and alkene (3 equiv.) in CH2Cl2 wasrefluxed; Ru catalyst (0.04 equiv.) was added; mixt. was stirred at ref lux over 24 h; solvent removed (vac.); chromd. (silica gel, cyclohexane/EtOAc, 19/1);
DOI:10.1016/j.jorganchem.2006.08.084