3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside
CAS No.:127588-82-3
Molecular Formula:C₅₈H₆₁NO₁₈
Molecular Weight:1060.12
Hs Code.:

3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of 3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

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Technology Process of 3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

There total 6 articles about 3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 105376-04-3,138661-53-7,113214-71-4
ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 127588-81-2
3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-L-glycero-α-D-manno-heptopyranoside

: 127588-82-3
3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With Phenylselenyl chloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; for 0.0833333h;

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 127588-82-3
3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: Hg(CN)2, HgBr₂ / acetonitrile / 4 h

2: Zemplen condition

3: p-toluenesulfonic acid / acetone / 1 h / 20 °C

4: 83 percent / benzeneselenyl chloride, 4 Angstroem molecular sieves, silver triflate / 1,2-dichloro-ethane / 0.08 h

With Phenylselenyl chloride; 4 A molecular sieve; silver trifluoromethanesulfonate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In 1,2-dichloro-ethane; acetone; acetonitrile;

Reference yield:

: 116302-67-1
2,3,4,6,7-penta-O-acetyl-L-glycero-α-D-manno-heptopyranosyl bromide

: 127588-82-3
3-(benzyloxycarbonylamino)propyl 2,3:6,7-di-O-isopropylidene-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: Hg(CN)2, HgBr₂ / acetonitrile / 4 h

2: Zemplen condition

3: p-toluenesulfonic acid / acetone / 1 h / 20 °C

4: 83 percent / benzeneselenyl chloride, 4 Angstroem molecular sieves, silver triflate / 1,2-dichloro-ethane / 0.08 h

With Phenylselenyl chloride; 4 A molecular sieve; silver trifluoromethanesulfonate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In 1,2-dichloro-ethane; acetone; acetonitrile;