N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester

Base Information

• Chemical Name: N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester
• CAS No.: 152843-96-4
• Molecular Formula: C₅₁H₅₁F₅N₂O₂₂
• Molecular Weight: 1138.96

Synonyms:

Chemical Property of N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester

There total 3 articles about N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Nα-(Fluoren-9-ylmethoxycarbonyl)-L-aspartic 4-Acid Chloride 1-pentafluorophenyl Ester (132785-38-7) + 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosylamine (30854-63-8,59044-96-1,93079-64-2,120575-75-9) → Nγ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-Nα-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester (152843-96-4)

Guidance literature:

With N-ethylmorpholine;; In tetrahydrofuran;

Reference yield:

tert-butyl N-[(9H-fluoren-9-ylmethoxy)carbonyl]-1-pentafluorophenyl L-aspartate (86061-01-0,200335-75-7) → Nγ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-Nα-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester (152843-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / trifluoroacetic acid, SOCl₂ / 24 h / 40 °C

2: 76 percent / N-ethylmorpholine / tetrahydrofuran

With N-ethylmorpholine;; thionyl chloride; trifluoroacetic acid; In tetrahydrofuran;

Reference yield:

2,3,6-tri-O-acetyl-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosylamine (152843-95-3) → Nγ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-Nα-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester (152843-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / piperidine / tetrahydrofuran / Ambient temperature

2: 76 percent / N-ethylmorpholine / tetrahydrofuran

With piperidine; N-ethylmorpholine;; In tetrahydrofuran;

upstream raw materials:

N^α-(Fluoren-9-ylmethoxycarbonyl)-L-aspartic 4-Acid Chloride 1-pentafluorophenyl Ester

2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosylamine

tert-butyl N-[(9H-fluoren-9-ylmethoxy)carbonyl]-1-pentafluorophenyl L-aspartate

2,3,6-tri-O-acetyl-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosylamine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 152843-96-4 N^γ-<2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-β-D-glucopyranosyl>-N^α-(fluoren-9-ylmethoxycarbonyl)-L-asparagine pentafluorophenyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send