chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate)

Base Information

• Chemical Name: chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate)
• CAS No.: 1207188-66-6
• Molecular Formula: C₂₀H₁₄N₅S*Cl*Pd
• Molecular Weight: 498.304
• Mol file: 1207188-66-6.mol

Synonyms:

Chemical Property of chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate)

There total 1 articles about chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-phenyl-3-phenyl-5-(benzothiazol-2-yl)formazan (21326-44-3,142399-45-9) + palladium dichloride → chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate) (1207188-66-6)

Guidance literature:

With HCl; In hydrogenchloride; toluene; soln. of 1,3-diphenyl-5-(benzothiazol-2-yl)formazan (1.1 mol) in tolueneadded to soln. of PdCl2 (1.5 mol) in dild. aq. HCl; mixt. stirred for 2 h; soln. stored at room temp. for 1 d; toluene layer sepd. and evapd.; solid dried; elem. anal.;

DOI:10.1134/S1070328409030099

Reference yield:

chloropalladium(II)(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate) (1207188-66-6) → dichlorobis(1,3-diphenyl-5-(benzothiazol-2-yl)formazanate)dipalladium(II)

Guidance literature:

With NH₄OH; In ethanol; several drops of concd. NH4OH added to soln. of complex in EtOH until color of soln. turned to blue; soln. evapd.;

DOI:10.1134/S1070328409030099

upstream raw materials:

1-phenyl-3-phenyl-5-(benzothiazol-2-yl)formazan