{(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

Base Information

Chemical Name:{(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru
CAS No.:112088-17-2
Molecular Formula:C₃₈H₃₁ClN₄PRu*ClO₄
Molecular Weight:810.638
Hs Code.:

{(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2{P(C<sub>6</sub>H<sub>5</sub>)3}RuCl}<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=C<sub>38</sub>H<sub>31</sub>Cl<sub>2</sub>N<sub>4</sub>PO<sub>4</sub>Ru

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Chemical Property of {(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

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Technology Process of {(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

There total 3 articles about {(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: sodium perchlorate

: 603-35-0
triphenylphosphine

: 112088-17-2
{(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

Guidance literature:: In ethanol; water; cis-Ru(bpy)2Cl2.2H2O and PPh3 in aq.EtOH refluxed 4-6 h, evapd. to dryness, H2O added, pptd. by excess NaClO4; filtered, purifn. by Al2O3/60:40 toluene/acetonitrile chromy., dissoln. in acetone and repptn. with ether;
DOI:10.1021/ja00213a019

Reference yield:

: 7601-90-3
perchloric acid

: cis-bis-(2,2′-bipyridine) dichlororuthenium(II) dihydrate

: 603-35-0
triphenylphosphine

: 112088-17-2
{(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

Guidance literature:: In ethanol; water; cis-Ru(bpy)2Cl2.2H2O and PPh3 in aq.EtOH refluxed 4-6 h, evapd. to dryness, H2O added, pptd. by 70% HClO4; filtered, purifn. by Al2O3/60:40 toluene/acetonitrile chromy., dissoln. in acetone and repptn. with ether;
DOI:10.1021/ja00213a019

Reference yield:

: 76549-23-0
cis-[Ru(2,2'-bipyridine)2(CO)Cl]ClO₄

: 112088-17-2
{(C₁₀H₈N₂)2{P(C₆H₅)3}RuCl}⁽¹⁺⁾*ClO₄^(1-)=C₃₈H₃₁Cl₂N₄PO₄Ru

Guidance literature:: With triphenylphosphine; In nitromethane; Irradiation (UV/VIS); room temp.; not isolated, detd. by spectr.;
DOI:10.1039/c39800000750