dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate

Base Information

• Chemical Name: dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate
• CAS No.: 292643-83-5
• Molecular Formula: C₅₉H₄₁N₈O₅Ru₂*F₆P
• Molecular Weight: 1289.13

Synonyms:

Chemical Property of dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate

There total 1 articles about dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

ammonium hexafluorophosphate + bis(2,2'-bipyridine)dichlororuthenium(II) dihydrate + fluorone black (975-17-7) → dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate (292643-83-5)

Guidance literature:

With AgNO₃; KOH; In ethanol; water; byproducts: AgCl; to Ru(bipy)2Cl2 AgNO3 was added, heated to reflux for 30 min, AgCl filtered, H3L and KOH added, heated to reflux for 2 h, EtOH evapd., NH4PF6 aq. soln. added, filtered, dried; chromy. on alumina.; UV, IR, NMR;

DOI:10.1039/b002563l

Reference yield:

dinuclear ruthenium(II)((bipy)2)(9-phenyl-2,3,7-trihydroxy-6-fluorone) hexafluorophosphate (292643-83-5) → [((NC5H4C5H4N)2Ru)2((O)2C6H2C(C6H5)C6H2(O)3)](2+)

Guidance literature:

In not given; recrystn. with aerial oxidn.; elem. anal.; UV, IR;

DOI:10.1039/b002563l

upstream raw materials:

fluorone black

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