2-phenyl-ethyl diazomethanesulfonate

Base Information

Chemical Name:2-phenyl-ethyl diazomethanesulfonate
CAS No.:866944-65-2
Molecular Formula:C₉H₁₀N₂O₃S
Molecular Weight:226.256
Hs Code.:

Synonyms:

Suppliers and Price of 2-phenyl-ethyl diazomethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-phenyl-ethyl diazomethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-phenyl-ethyl diazomethanesulfonate

There total 2 articles about 2-phenyl-ethyl diazomethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,3,3-trifluoro-2-oxo-propane-1-sulfonic acid 2-phenylethyl ester

: 866944-65-2
2-phenyl-ethyl diazomethanesulfonate

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; water; triethylamine; In acetonitrile; at 20 ℃;
DOI:10.1039/b412285b

Reference yield:

: 20020-27-3
2-phenylethyl mesylate

: 866944-65-2
2-phenyl-ethyl diazomethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiHMDS / tetrahydrofuran / 0.5 h / -78 °C

1.2: tetrahydrofuran / 0.17 h / -78 °C

2.1: 4-acetamidobenzenesulfonyl azide; Et₃N; water / acetonitrile / 20 °C

With 4-acetamidobenzenesulfonyl azide; water; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; acetonitrile;
DOI:10.1039/b412285b