benzyldimethyl(2-phenylethyl)stannane

Base Information

Chemical Name:benzyldimethyl(2-phenylethyl)stannane
CAS No.:153771-94-9
Molecular Formula:C₁₇H₂₂Sn
Molecular Weight:345.072
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyldimethyl(2-phenylethyl)stannane

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Technology Process of benzyldimethyl(2-phenylethyl)stannane

There total 2 articles about benzyldimethyl(2-phenylethyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 622-24-2
2-phenylethyl chloride

: 153771-95-0
C₆H₅CH₂(CH₃)2SnBr

: 153771-94-9
benzyldimethyl(2-phenylethyl)stannane

Guidance literature:: With magnesium; In diethyl ether; N2 atmosphere; dropwise addn. of mixt. of 2-phenylethyl chloride and Mg in ether to soln. of PhCH2SnMe2Br (stirring), refluxing (14 h), hydrolysis (pH=7.0, room temp.); washing (water), drying of org. phase (over MgSO4), removal of solvent (distn.), fractional distn. of residue;
DOI:10.1016/0022-328X(93)80293-K

Reference yield:

: 17841-75-7
dibenzyldimethylstannane

: 153771-94-9
benzyldimethyl(2-phenylethyl)stannane

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / tetrachloromethane

2: magnesium / diethyl ether

With bromine; magnesium; In tetrachloromethane; diethyl ether;
DOI:10.1016/0022-328X(93)80293-K