tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate]

Base Information

Chemical Name:tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate]
CAS No.:85041-23-2
Molecular Formula:C₂₄H₂₀P*C₄₉H₄₉N₂O₂Re₂S₇
Molecular Weight:1634.21
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate]

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Technology Process of tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate]

There total 1 articles about tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 83095-49-2
bis(triphenylphosphane)methoxydichloronitrosylrhenium

: 2751-90-8
tetraphenylphosphonium bromide

: 106-45-6
para-thiocresol

: 85041-23-2
tetraphenylphosphonium tri-μ-4-methylthiophenolato-bis[di-(4-methylthiophenolato)nitrosylrhenate]

Guidance literature:: With (C₂H₅)3N; In methanol; to a suspn. of Re-compd. in MeOH were added (under N2) 4-methylthiophenol and (C2H5)3N; the mixt. was heated under reflux for 1 h; the cooled soln. was filtered and treated with (PPh4)Br;; the ppt. was washed with Pr(i)OH and diethyl ether; recrystn. from CH2Cl2-diethyl ether; elem. anal.;;