16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene

Base Information

Chemical Name:16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene
CAS No.:117696-92-1
Molecular Formula:C₁₈H₁₆O
Molecular Weight:248.324
Hs Code.:
DSSTox Substance ID:DTXSID10151875
Nikkaji Number:J1.029.884I
Wikidata:Q83018421
Mol file:117696-92-1.mol

Synonyms:16,17-dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene;16,17-DMCPA

Suppliers and Price of 16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
16,17-DIHYDRO-11-METHOXY-15H-CYCLOPENTA(A)PHENANTHRENE 95.00%
5MG
$ 503.56

Total 1 raw suppliers

Chemical Property of 16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene

Chemical Property:

Vapor Pressure:1.11E-07mmHg at 25°C
Boiling Point:444.6°Cat760mmHg
Flash Point:182°C
PSA：9.23000
Density:1.178g/cm³
LogP:4.49030
XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:248.120115130
Heavy Atom Count:19
Complexity:326

Purity/Quality:: 16,17-DIHYDRO-11-METHOXY-15H-CYCLOPENTA(A)PHENANTHRENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C2C(=C3CCCC3=C1)C=CC4=CC=CC=C42

Technology Process of 16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene

There total 6 articles about 16,17-Dihydro-11-methoxy-15H-cyclopenta(a)phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sulfuric acid mono-(11-methoxy-16,17-dihydro-15H-cyclopenta[a]phenanthren-17-yl) ester

: 117696-92-1
16,17-dihydro-11-methoxy-15H-cyclopenta[a]phenanthrene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S1383-5718(99)00215-6

Reference yield:

: 83053-63-8
15,16-dihydro-11-hydroxycyclopenta[a]phenanthrene

: 117696-92-1
16,17-dihydro-11-methoxy-15H-cyclopenta[a]phenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 6.6 g / K₂CO₃ / acetonitrile / 72 h / Ambient temperature

2: sodium borohydride / methanol

3: 1.05 g / H₂, conc. aq. HCl, glacial acetic acid / 5 percent Pd/C

With hydrogenchloride; sodium tetrahydroborate; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; acetonitrile;

Reference yield:

: 24684-58-0
11-acetoxy-15,16-dihydrocyclopenta phenanthren-17-one

: 117696-92-1
16,17-dihydro-11-methoxy-15H-cyclopenta[a]phenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: 7.5 g / KOH, methanol / 48 h / Ambient temperature

2: 6.6 g / K₂CO₃ / acetonitrile / 72 h / Ambient temperature

3: sodium borohydride / methanol

4: 1.05 g / H₂, conc. aq. HCl, glacial acetic acid / 5 percent Pd/C

With hydrogenchloride; methanol; potassium hydroxide; sodium tetrahydroborate; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; acetonitrile;