BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)

Base Information

Chemical Name:BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)
CAS No.:833462-58-1
Molecular Formula:C₂₅H₂₅B₃N₂O₅
Molecular Weight:465.917
Hs Code.:

BOB(OB(C<sub>6</sub>H<sub>5</sub>)O)(OC<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)NCH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>NC(CH<sub>3</sub>)C<sub>6</sub>H<sub>4</sub>O)

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Suppliers and Price of BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)

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Technology Process of BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)

There total 1 articles about BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 54216-01-2
bis-N,N'-(2-hydroxyacetophenylidine)-1,3-propanediamine

: 11113-50-1,14635-83-7
boric acid

: 98-80-6
phenylboronic acid

: 833462-58-1
BOB(OB(C₆H₅)O)(OC₆H₄C(CH₃)NCH₂CH₂CH₂NC(CH₃)C₆H₄O)

Guidance literature:: In acetonitrile; soln. of Schiff base (1 equiv.) and H3BO3 (2 equiv.) in acetonitrile refluxed until yellow ppt. formed, 1 equiv. of phenylboronic acid added, mixt. refluxed for 4 h using a Dean-Stark trap; ppt. filtered off, dried; elem. anal.;
DOI:10.1021/ic048862e