(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

Base Information

Chemical Name:(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester
CAS No.:98889-85-1
Molecular Formula:C₄₀H₃₂N₄O₈
Molecular Weight:696.716
Hs Code.:

(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

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Chemical Property of (5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

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Technology Process of (5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

There total 7 articles about (5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98889-67-9
dibenzhydryl 6-chloro-6-deaminogriseolate

: 98889-85-1
(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

Guidance literature:: With zinc; In water; acetic acid; for 4h; Ambient temperature;
DOI:10.1248/cpb.36.1309

Reference yield:

: 98871-07-9
dibenzhydryl griseolate

: 98889-85-1
(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / sodium nitrit / acetic acid; H₂O

2: 80 percent / pyridine / 3 h / Ambient temperature

3: 82 percent / phosphorus oxychloride, N,N-diethylaniline / ethyl acetate / 0.05 h / Heating

4: 83 percent / ammonia / methanol / 0.83 h / Ambient temperature

5: Zn / acetic acid; H₂O / 4 h / Ambient temperature

With pyridine; ammonia; N,N-diethylaniline; zinc; sodium nitrite; trichlorophosphate; In methanol; water; acetic acid; ethyl acetate;
DOI:10.1248/cpb.36.1309

Reference yield:

: 79030-08-3,99146-56-2
griseolic acid

: 98889-85-1
(5R,6R)-2-(Benzhydryloxycarbonyl-hydroxy-methyl)-6-hydroxy-5-purin-9-yl-2,5,6,6a-tetrahydro-furo[3,2-b]furan-2-carboxylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / acetone; H₂O / 16 h / Ambient temperature

2: 100 percent / sodium nitrit / acetic acid; H₂O

3: 80 percent / pyridine / 3 h / Ambient temperature

4: 82 percent / phosphorus oxychloride, N,N-diethylaniline / ethyl acetate / 0.05 h / Heating

5: 83 percent / ammonia / methanol / 0.83 h / Ambient temperature

6: Zn / acetic acid; H₂O / 4 h / Ambient temperature

With pyridine; ammonia; N,N-diethylaniline; zinc; sodium nitrite; trichlorophosphate; In methanol; water; acetic acid; ethyl acetate; acetone;
DOI:10.1248/cpb.36.1309