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Technology Process of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2

CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2

Base Information
  • Chemical Name:CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2
  • CAS No.:1082577-58-9
  • Molecular Formula:C37H32BNS2
  • Molecular Weight:565.611
  • Hs Code.:
CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>B(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)C<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2
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Technology Process of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2

There total 1 articles about CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-trimethylstannyl-5'-diphenylamino-2,2'-bithiophene

5-trimethylstannyl-5'-diphenylamino-2,2'-bithiophene

CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>BBrC<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>C<sub>6</sub>H<sub>13</sub>
1082577-52-3

CH2CHC6H4BBrC4H2S2C4H2C6H13

(Cu(mesitylene))*(Toluene)<sub>0.2</sub>

(Cu(mesitylene))*(Toluene)0.2

CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>B(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)C<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>5</sub>)2
1082577-58-9

CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2N(C6H5)2

Guidance literature:
In dichloromethane; BBr3 in CH2Cl2 was added dropwise to polystyrene in CH2Cl2, stirred at room temp., Sn-compound in CH2Cl2 was added, stirred, evapd., Cu-compoundin toluene was added dropwise to B-compound in toluene, 130°C; filtered through celite, concd., pptd. into cold hexane, repeated pptn. from toluene into hexane, dried;
DOI:10.1021/ja063302v
upstream raw materials:

CH2CHC6H4BBrC4H2S2C4H2C6H13

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