(μ-Li(OEt2))[PhB(μ-NtBu)2]2Al

Base Information

• Chemical Name: (μ-Li(OEt2))[PhB(μ-NtBu)2]2Al
• CAS No.: 865817-73-8
• Molecular Formula: C₃₂H₅₆AlB₂LiN₄O
• Molecular Weight: 568.367
• Mol file: 865817-73-8.mol

Synonyms:

Chemical Property of (μ-Li(OEt2))[PhB(μ-NtBu)2]2Al

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (μ-Li(OEt2))[PhB(μ-NtBu)2]2Al

There total 1 articles about (μ-Li(OEt2))[PhB(μ-NtBu)2]2Al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

([PhB(μ-N(t)Bu)2]AlCl(OEt2)) (865817-72-7) + bis(tert-butylamino)phenylborane dilithium salt (124652-56-8) → (μ-Li(OEt2))[PhB(μ-NtBu)2]2Al (865817-73-8)

Guidance literature:

In diethyl ether; benzene; 1 equiv. of ligand treated with 1 equiv. of Al complex in boiling benzene/Et2O;

DOI:10.1039/b506253e

Reference yield:

(μ-Li(OEt2))[PhB(μ-NtBu)2]2Al (865817-73-8) → [PhB(μ-NtBu)2]2Al

Guidance literature:

With I₂; In diethyl ether; Al complex treated with iodine; crystd. in Et2O at 258 K;

DOI:10.1039/b506253e

upstream raw materials:

([PhB(μ-N(t)Bu)2]AlCl(OEt2))

bis(tert-butylamino)phenylborane dilithium salt