(C₆H₅C(NSi(CH₃)3)2)GeCl

Base Information

Chemical Name:(C₆H₅C(NSi(CH₃)3)2)GeCl
CAS No.:1233957-92-0
Molecular Formula:C₁₃H₂₃ClGeN₂Si₂
Molecular Weight:371.553
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>C(NSi(CH<sub>3</sub>)3)2)GeCl

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Chemical Property of (C₆H₅C(NSi(CH₃)3)2)GeCl

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Technology Process of (C₆H₅C(NSi(CH₃)3)2)GeCl

There total 1 articles about (C₆H₅C(NSi(CH₃)3)2)GeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: germanium(II) chloride dioxane

: lithium N,N'-bis(trimethylsilyl)benzamidinate

: 1233957-92-0
(C₆H₅C(NSi(CH₃)3)2)GeCl

Guidance literature:: In diethyl ether; under Ar; soln. of freshly prepared Li compd. in Et2O added to suspn. ofGe compd. in Et2O at -78°C; warmed to room temp.; stirred for 2. 5 h; refluxed for 4 h; solvent removed under reduced pressure; extd. with toluene; filtered throug Celite; filtrate concd. in vac.; solid obtained; elem. anal.;
DOI:10.1021/om100347c

Reference yield: 99.0%

: 1233957-92-0
(C₆H₅C(NSi(CH₃)3)2)GeCl

: bis(tris(trimethylsilyl)stannyl)magnesium*2THF

: C₆H₅C(NSi(CH₃)3)2GeSn(Si(CH₃)3)3

Guidance literature:: In tetrahydrofuran; byproducts: MgCl2; (Ar); using Schlenk techniques; addn. of soln. of bis(tris(trimethylsilyl)stannyl)magnesium in THF to soln. of PhC(NSiMe3)2GeCl (2 equiv.) in THF at -78°C for 45 min, warming to room temp., stirring for 20 h; removal of solvent under vac., extn. with pentane, filtration, concn., cooling at -24°C, crystn. from satd. soln. of pentane at -24°C;
DOI:10.1021/om200024d

Reference yield: 96.0%

: 1233957-92-0
(C₆H₅C(NSi(CH₃)3)2)GeCl

: bis(tris(trimethylsilyl)germyl)magnesium*2THF

: 1285511-68-3
C₆H₅C(NSi(CH₃)3)2GeGe(Si(CH₃)3)3

Guidance literature:: In tetrahydrofuran; byproducts: MgCl2; (Ar); using Schlenk techniques; addn. of soln. of bis(tris(trimethylsilyl)germyl)magnesium in THF to soln. of PhC(NSiMe3)2GeCl (2 equiv.) in THFat -78°C for 45 min, warming to room temp., stirring for 20 h; removal of solvent under vac., extn. with pentane, filtration, concn., cooling at -24°C, crystn. from satd. soln. of pentane at -24°C;
DOI:10.1021/om200024d