Technology Process of C30H30O8
There total 11 articles about C30H30O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium bromide; TEMPO; NaOCl / sodium acetate; bleach / ethyl acetate; H2O / 14 - 20 °C
2: 7.02 kg / toluene; tetrahydrofuran / 1.83 h / -10 - 0 °C
3: 10.81 kg / Triton X-405; KOH / toluene; H2O / 20 h / Heating
4: 9.02 kg / aq. sulfuric acid / toluene; acetonitrile / 19 °C
5: pyridine / acetonitrile / 12 h / 50 - 55 °C
6: aq. HBF4 / acetonitrile / 2 h / 50 - 55 °C
7: periodic acid / H2O / 0.5 h / 0 - 5 °C
With
pyridine; 2,2,6,6-tetramethyl-piperidine-N-oxyl; potassium hydroxide; sodium hypochlorite; tetrafluoroboric acid; sulfuric acid; Triton X-114; periodic acid; sodium bromide;
sodium hypochlorite; sodium acetate;
In
tetrahydrofuran; water; ethyl acetate; toluene; acetonitrile;
DOI:10.1021/jo0491096
- Guidance literature:
-
With
periodic acid;
In
water;
at 0 - 5 ℃;
for 0.5h;
Title compound not separated from byproducts;
DOI:10.1021/jo0491096
- Guidance literature:
-
With
periodic acid;
In
acetonitrile;
at 0 - 5 ℃;
for 0.5h;
DOI:10.1021/jo049121y