N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

Base Information

Chemical Name:N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)
CAS No.:1400696-71-0
Molecular Formula:C₂₂H₁₈N₈O₂
Molecular Weight:426.437
Hs Code.:

Synonyms:

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Chemical Property of N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

Chemical Property:

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Technology Process of N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

There total 3 articles about N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 539-48-0
p-xylylidenediamine

: 39986-42-0
3-azidobenzoyl chloride

: 1400696-71-0
N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2ob26272j

Reference yield:

: 1843-35-2
3-azidobenzoic acid

: 1400696-71-0
N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: sodium carbonate / dichloromethane; water / 18 h / 20 °C / Inert atmosphere

With oxalyl dichloride; sodium carbonate; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1039/c2ob26272j

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 1400696-71-0
N,N'-(1,4-phenylenebis(methylene))bis(3-azidobenzamide)

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(ll) sulfate pentahydrate / methanol / 18 h / 20 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: sodium carbonate / dichloromethane; water / 18 h / 20 °C / Inert atmosphere

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; oxalyl dichloride; sodium carbonate; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1039/c2ob26272j