C₁₅H₂₀O₃

Base Information

• Chemical Name: C₁₅H₂₀O₃
• CAS No.: 1160960-89-3
• Molecular Formula: C₁₅H₂₀O₃
• Molecular Weight: 248.322
• Mol file: 1160960-89-3.mol

Synonyms:

Chemical Property of C₁₅H₂₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₂₀O₃

There total 7 articles about C₁₅H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H20O2 (1160960-86-0) → C15H20O3 (1160960-89-3)

Guidance literature:

Multi-step reaction with 3 steps

1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.25 h / 20 °C

3: diethyl ether

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; In diethyl ether; dichloromethane; water; tert-butyl alcohol;

DOI:10.1021/jm201685h

Reference yield:

3-[(benzyloxy)methyl]hex-5-enal (1160960-87-1) → C15H20O3 (1160960-89-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.25 h / 20 °C

2: diethyl ether

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In diethyl ether; water; tert-butyl alcohol;

DOI:10.1021/jm201685h

Reference yield:

4-carbomethoxy-6-t-butyldimethylsiloxy-1-hexene (123453-82-7) → C15H20O3 (1160960-89-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; hexanes / -10 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 12 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

5.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.25 h / 20 °C

6.1: diethyl ether

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; hexanes; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

DOI:10.1021/jm201685h

upstream raw materials:

C₁₄H₁₈O₃

diazomethyl-trimethyl-silane

C₁₄H₂₀O₂

3-[(benzyloxy)methyl]hex-5-enal

Downstream raw materials:

C₁₈H₂₄O₅