C₄₉H₅₂N₄O₈

Base Information

Chemical Name:C₄₉H₅₂N₄O₈
CAS No.:1373501-80-4
Molecular Formula:C₄₉H₅₂N₄O₈
Molecular Weight:824.974
Hs Code.:

C<sub>49</sub>H<sub>52</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₄₉H₅₂N₄O₈

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Technology Process of C₄₉H₅₂N₄O₈

There total 13 articles about C₄₉H₅₂N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94341-55-6
(4-(aminomethyl)phenyl)(phenyl)methanone

: 1373501-80-4
C₄₉H₅₂N₄O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere

1.2: 2 h / Inert atmosphere

2.1: triethylamine; trichlorophosphate / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice

3.1: methanol; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.2: 9 h / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trichlorophosphate; In methanol; dichloromethane; N,N-dimethyl-formamide; 3.1: Ugi reaction / 3.2: Ugi reaction;
DOI:10.1039/c2cc31294h

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1373501-80-4
C₄₉H₅₂N₄O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / acetonitrile / 1 h / 50 °C / Inert atmosphere

2.1: sodium methylate / methanol / 24 h / Reflux; Inert atmosphere

3.1: hydroxylamine monohydrate; toluene-4-sulfonic acid / methanol / 24 h / Reflux

4.1: lithium hydroxide / methanol; water / 2 h / Cooling with ice

5.1: pyridine; trichlorophosphate / chloroform / 1 h / Inert atmosphere

6.1: ozone / dichloromethane / -78 °C

7.1: methanol; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

7.2: 9 h / 20 °C / Inert atmosphere

8.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

With pyridine; hydroxylamine monohydrate; sodium methylate; potassium carbonate; toluene-4-sulfonic acid; ozone; trifluoroacetic acid; lithium hydroxide; trichlorophosphate; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile; 7.1: Ugi reaction / 7.2: Ugi reaction;
DOI:10.1039/c2cc31294h

Reference yield:

: 1373502-18-1
methyl 5-(4-(allyloxy)phenyl)isoxazole-3-carboxylate

: 1373501-80-4
C₄₉H₅₂N₄O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide / methanol; water / 2 h / Cooling with ice

2.1: pyridine; trichlorophosphate / chloroform / 1 h / Inert atmosphere

3.1: ozone / dichloromethane / -78 °C

4.1: methanol; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4.2: 9 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

With pyridine; ozone; trifluoroacetic acid; lithium hydroxide; trichlorophosphate; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 4.1: Ugi reaction / 4.2: Ugi reaction;
DOI:10.1039/c2cc31294h