pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride

Base Information

Chemical Name:pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride
CAS No.:663606-89-1
Molecular Formula:C₂₃H₂₈ClLuS
Molecular Weight:546.961
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride

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Technology Process of pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride

There total 1 articles about pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 40585-51-1
pentamethylcyclopentadienyl sodium

: 24614-69-5,144491-06-5,120496-88-0
LuCl₃(THF)3

: 663606-24-4
2-phenylthioethylcyclopentadienylsodium

: 663606-89-1
pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; all manipulations under inert atm. of N2 or Ar; S compd. added to suspn.of lanthanoide compd. in THF at room temp, then NaC5Me5 added, stirred for 12 h; solvent removed in vac., residue washed with n-hexane, extd. with toluene, concd. in vac., cooled to -28°C for crystn., elem. anal.;

Reference yield: 48.0%

: 663606-89-1
pentamethylcyclopentadienyl(2-phenylthioethylcyclopentadienyl)lutetium chloride

: 917-54-4
methyllithium

: 663606-94-8
methyl(pentamethylcyclopentadienyl)(2-phenylthioethylcyclopentadienyl)lutetium

Guidance literature:: In diethyl ether; toluene; byproducts: LiCl; all manipulations under inert atm. of N2 or Ar; soln. of MeLi in Et2O added to soln. of lanthanoide compd. in toluene at -78°C, stirred at room temp. for 2 d; filtered, concd. in vac., cooled to -28°C for crystn., elem. anal.;