[CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

Base Information

Chemical Name:[CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]
CAS No.:1220139-92-3
Molecular Formula:C₂₂H₂₂B₂ClCuN₇
Molecular Weight:505.085
Hs Code.:

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Chemical Property of [CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

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Technology Process of [CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

There total 3 articles about [CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: [Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph]

: copper dichloride

: 1220139-92-3
[CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

Guidance literature:: With n-C₄H₉Li; In tetrahydrofuran; hexane; byproducts: LiCl; under N2 atm. using Schlenk techniques; mixt. of borate ligand and CuCl2in THF was stirred at room temp. for 2 h; cooled to -78°C; soln. of n-BuLi in hexane added; mixt. allowed to warm to room temp.; stirred for 2 h; layered with hexane; crystals are formed; collected on a frit; rinsed with hexane; crystals dried (vac.); elem. anal.;
DOI:10.1021/ic100104t

Reference yield:

: 105336-05-8
((CH₃)2N(C₆H₅)B)2NCH₃

: 1220139-92-3
[CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: n-C₄H₉Li / tetrahydrofuran; hexane

With n-C₄H₉Li; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ic100104t

Reference yield:

: 16548-71-3
bromo-(dimethylamino)phenyl borane

: 1220139-92-3
[CuCl[Ph(pyrazol-1-yl)B(μ-NH(Me))(μ-pyrazol-1-yl)B(pyrazol-1-yl)Ph(-1H)]]

Guidance literature:: Multi-step reaction with 3 steps

1: pentane

2: diethyl ether

3: n-C₄H₉Li / tetrahydrofuran; hexane

With n-C₄H₉Li; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/ic100104t