C₁₃H₁₇Br

Base Information

• Chemical Name: C₁₃H₁₇Br
• CAS No.: 1350431-01-4
• Molecular Formula: C₁₃H₁₇Br
• Molecular Weight: 253.182
• Mol file: 1350431-01-4.mol

Synonyms:

Chemical Property of C₁₃H₁₇Br

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₇Br

There total 1 articles about C₁₃H₁₇Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

4-Methyl-1-pentene (691-37-2,25068-26-2) + 3-bromobenzyl chloride (932-77-4) → C13H17Br (1350431-01-4)

Guidance literature:

4-Methyl-1-pentene; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; triethylamine; dicyclohexylphenylphosphine; at 20 ℃; for 0.0833333h; Inert atmosphere; Sealed tube; neat (no solvent);

3-bromobenzyl chloride; With triethylsilyl trifluoromethyl sulfonate; at 20 ℃; for 16h; regioselective reaction; Inert atmosphere; Sealed tube; neat (no solvent);

DOI:10.1021/ja209235d

upstream raw materials:

4-Methyl-1-pentene

3-bromobenzyl chloride