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C19H25NO5

Base Information
  • Chemical Name:C19H25NO5
  • CAS No.:1379449-83-8
  • Molecular Formula:C19H25NO5
  • Molecular Weight:347.411
  • Hs Code.:
C<sub>19</sub>H<sub>25</sub>NO<sub>5</sub>

Synonyms:

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Chemical Property of C19H25NO5
Chemical Property:
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Technology Process of C19H25NO5

There total 6 articles about C19H25NO5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 25 ℃; for 12h;
DOI:10.1021/ja301326k
Guidance literature:
Multi-step reaction with 2 steps
1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere
2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja301326k
Guidance literature:
Multi-step reaction with 6 steps
1.1: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1.5 h / -15 °C / Inert atmosphere
2.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 25 °C / Darkness
3.1: iodine; zinc / N,N-dimethyl-formamide / 0.75 h / Inert atmosphere
3.2: 16 h / 60 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
4.2: 6 h / 0 °C
5.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere
6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C
With 4-methyl-morpholine; 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; iodine; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; zinc; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja301326k
upstream raw materials:

C18H28N2O6

C21H32N2O6

C21H29NO5

C10H19IN2O4

Downstream raw materials:

C26H31NO6

C27H30F3NO8S

C22H22F3NO6S

C38H49NO6Si

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