({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

Base Information

Chemical Name:({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate
CAS No.:139609-74-8
Molecular Formula:BF₄*C₄₅H₅₅NO₄P₂Rh
Molecular Weight:925.594
Hs Code.:

({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

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Chemical Property of ({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

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Technology Process of ({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

There total 1 articles about ({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate

: 139609-63-5
{PS,3R,4R,P'S}-1-(t-butoxycarbonyl)-3,4-bis-((2-methoxybenzyl)phenylphosphanyl)pyrrolidine

: 139609-74-8
({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

Guidance literature:: In methanol; Ar atmosphere; drying of org. compd. (2 d, 45°C, vac.), dissoln. (MeOH), cooling (-25°C), addn. of Rh-compd.; partial evapn., addn. of Et2O, filtration, washing (Et2O), drying (vac.); elem. anal.;

Reference yield:

: 139609-74-8
({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')(1,5-cyclooctadiene)rhodium tetrafluoroborate

: ({PR,3R,4R,P'R}-1-(tert-butoxycarbonyl)-3,4-bis{(2-methoxybenzyl)phenylphosphanyl}pyrrolidine-P,P')rhodium tetrafluoroborate

Guidance literature:: With H₂; In d⁽⁴⁾-methanol; Ar atmosphere; dissoln. in CD3OD (NMR tube), stirring (H2, 12 h, exclusion of light); not isolated; (31)P-NMR spectroscopy;