C₆H₅Ge(C₂C₆H₅)3

Base Information

• Chemical Name: C₆H₅Ge(C₂C₆H₅)3
• CAS No.: 96376-65-7
• Molecular Formula: C₃₀H₂₀Ge
• Molecular Weight: 453.079
• Mol file: 96376-65-7.mol

Synonyms:

Chemical Property of C₆H₅Ge(C₂C₆H₅)3

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₆H₅Ge(C₂C₆H₅)3

There total 1 articles about C₆H₅Ge(C₂C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

germaniumtetrachloride (10038-98-9) + phenylacetylene (536-74-3) → C6H5Ge(C2C6H5)3 (96376-65-7)

Guidance literature:

With ZnCl₂; triethylamine; HCl; In 1,4-dioxane; mixt. of ZnCl2 and dioxane heated to 85-90°C, triethylamine and ligand added, after 10 min GeCl4 added, kept at 100°C for 3.5 h, treated with HCl; ppt. extd. with CHCl3, dried with CaCl2, concd., column chromy. on silica gel with CHCl3, crystd. slowly;

DOI:10.1007/s11172-006-0434-5

upstream raw materials:

germaniumtetrachloride

phenylacetylene