C₂₂H₂₉FN₂O₂

Base Information

Chemical Name:C₂₂H₂₉FN₂O₂
CAS No.:1391848-21-7
Molecular Formula:C₂₂H₂₉FN₂O₂
Molecular Weight:372.483
Hs Code.:

C<sub>22</sub>H<sub>29</sub>FN<sub>2</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₂₂H₂₉FN₂O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₂₉FN₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₂₉FN₂O₂

There total 5 articles about C₂₂H₂₉FN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391848-34-2
C₂₂H₂₇FN₄O₂

: 1391848-21-7
C₂₂H₂₉FN₂O₂

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2012.06.059

Reference yield:

: 259543-80-1
ethyl 2-(3-fluoro-4-hydroxyphenyl)acetate

: 1391848-21-7
C₂₂H₂₉FN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / acetone / Reflux

2: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / 6 h / Reflux

3: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

4: water; sodium hydroxide / 2 h / Reflux

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

6: palladium on activated charcoal; hydrogen / methanol / 20 °C

With dmap; sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; water; hydrogen; sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.bmcl.2012.06.059

Reference yield:

: 1391848-23-9
C₁₂H₁₄FN₃O₃

: 1391848-21-7
C₂₂H₂₉FN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

2: water; sodium hydroxide / 2 h / Reflux

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

4: palladium on activated charcoal; hydrogen / methanol / 20 °C

With dmap; palladium on activated charcoal; water; hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.06.059