antimony(III) m-cresoxydichloride

Base Information

Chemical Name:antimony(III) m-cresoxydichloride
CAS No.:92919-89-6
Molecular Formula:C₇H₇Cl₂OSb
Molecular Weight:299.788
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of antimony(III) m-cresoxydichloride

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Technology Process of antimony(III) m-cresoxydichloride

There total 1 articles about antimony(III) m-cresoxydichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1807-38-1
SbCl₃(CH₃C₆H₄OH)

: 92919-89-6
antimony(III) m-cresoxydichloride

Guidance literature:: In chloroform; byproducts: HCl; dry atmosphere, thin slurry of the adduct in CHCl3 slowly heated to ca 60°C, evolution of HCl gas, addn. of a few drops of CHCl3 from time to time, further heating up to the end of HCl fuming; cooling, extn. (ether, benzene, chloroform), evapn. to dryness (reducedpressure), washing (petroleum ether), drying, elem. anal.;

Reference yield:

: 92919-89-6
antimony(III) m-cresoxydichloride

: 92922-89-9
dicyclopentadienylantimony(III) m-cresoxide

Guidance literature:: With NaC₅H₅; In tetrahydrofuran; dry atmosphere, addn. of a NaC5H5 soln. to a soln. of the dichloride inTHF in 2 : 1 molar ratio, refluxing for 4 - 6 h; cooling, filtering (G-4 sintered glass disc), dark colored mother liquor, distn. off (reduced pressure), recrystn. (THF/ether), elem. anal.;