C₂₈H₃₅ClN₄O₅

Base Information

Chemical Name:C₂₈H₃₅ClN₄O₅
CAS No.:1266683-67-3
Molecular Formula:C₂₈H₃₅ClN₄O₅
Molecular Weight:543.063
Hs Code.:

C<sub>28</sub>H<sub>35</sub>ClN<sub>4</sub>O<sub>5</sub>

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Chemical Property of C₂₈H₃₅ClN₄O₅

Chemical Property:

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Technology Process of C₂₈H₃₅ClN₄O₅

There total 17 articles about C₂₈H₃₅ClN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₆N₄O₆

: 1266683-67-3
C₂₈H₃₅ClN₄O₅

Guidance literature:: With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201001560

Reference yield:

: 1266683-59-3
N-Boc-3-bromo-5-isobutoxyaniline

: 1266683-67-3
C₂₈H₃₅ClN₄O₅

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine / 48 h / 78 °C / Inert atmosphere

2: sodium hydride / toluene / 1 h / Reflux

3: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 32 °C / Inert atmosphere; Darkness

4: water; sodium hydroxide / tetrahydrofuran / 5 h / 20 °C

5: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water; sodium hydride; copper(II) sulfate; sodium L-ascorbate; diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol; 1: Sonogashira coupling;
DOI:10.1002/chem.201001560

Reference yield:

: 1266683-62-8
N-Boc-3-ethynyl-5-isobutoxyaniline

: 1266683-67-3
C₂₈H₃₅ClN₄O₅

Guidance literature:: Multi-step reaction with 3 steps

1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 32 °C / Inert atmosphere; Darkness

2: water; sodium hydroxide / tetrahydrofuran / 5 h / 20 °C

3: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 20 °C

With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; water; copper(II) sulfate; sodium L-ascorbate; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/chem.201001560