Technology Process of C27H18O9
There total 5 articles about C27H18O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C30H24O9;
With
potassium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran; water;
DOI:10.1039/c2cc34938h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
3.1: boron tribromide / dichloromethane / -78 °C / Inert atmosphere
3.2: Reflux
4.1: potassium hydroxide / tetrahydrofuran / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; boron tribromide; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc34938h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / -78 °C / Inert atmosphere
2.2: Reflux
3.1: potassium hydroxide / tetrahydrofuran / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); boron tribromide; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc34938h
