Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate)

Base Information

• Chemical Name: Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate)
• CAS No.: 157378-10-4
• Molecular Formula: C₂₈H₁₆F₆N₂O₄Pd
• Molecular Weight: 664.856
• Mol file: 157378-10-4.mol

Synonyms:

Chemical Property of Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate)

There total 2 articles about Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(4,7-diphenyl-1,10-phenanthroline)palladium(II) acetate (95246-09-6) + trifluoroacetic acid (76-05-1) → Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate) (157378-10-4)

Guidance literature:

In methanol; the Pd-complex is dissolved in MeOH at room temp., sol. is filtd. and anexcess of CF3COOH added; ppt. is filtd. of, washed with cold MeOH and dried in vac., elem. anal.;

DOI:10.1039/DT9940001903

Reference yield:

bathophenanthroline (1662-01-7) → Pd (4,7-diphenyl-1,10-phenantroline) bis(trifluoroacetate) (157378-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₃COOH / acetone

2: methanol

With CH₃COOH; In methanol; acetone;

DOI:10.1039/DT9940001903

upstream raw materials:

(4,7-diphenyl-1,10-phenanthroline)palladium(II) acetate

trifluoroacetic acid

bathophenanthroline