[Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

Base Information

Chemical Name:[Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]
CAS No.:952100-89-9
Molecular Formula:C₃₄H₂₈N₁₀NiS₂
Molecular Weight:699.485
Hs Code.:

[Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone<sup>(1-)</sup>)2]

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Chemical Property of [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

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Technology Process of [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

There total 1 articles about [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 952100-91-3
(E)-2-((1,3-diphenyl-1H-pyrazol-4-yl)methylene)hydrazine-1-carbothioamide

: 6018-89-9
nickel(II) acetate tetrahydrate

: 952100-89-9
[Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

Guidance literature:: In methanol; acetone; Ni(CH3COO)2*4H2O dissolved in methanol under heating and the soln. mixedwith a warm soln. of the organic ligand in acetone; heating continued f or several minutes; left standing for 10 h; crystals filtered and washed with acetone and dried over anhydrous calcium chloride; elem. anal.;
DOI:10.1016/j.poly.2007.04.012