[Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

Base Information

• Chemical Name: [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]
• CAS No.: 952100-89-9
• Molecular Formula: C₃₄H₂₈N₁₀NiS₂
• Molecular Weight: 699.485
• Mol file: 952100-89-9.mol

Synonyms:

Chemical Property of [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2]

There total 1 articles about [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone^(1-))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

(E)-2-((1,3-diphenyl-1H-pyrazol-4-yl)methylene)hydrazine-1-carbothioamide (952100-91-3) + nickel(II) acetate tetrahydrate (6018-89-9) → [Ni(1,3-diphenylpyrazole-4-carboxaldehyde thiosemicarbazone(1-))2] (952100-89-9)

Guidance literature:

In methanol; acetone; Ni(CH3COO)2*4H2O dissolved in methanol under heating and the soln. mixedwith a warm soln. of the organic ligand in acetone; heating continued f or several minutes; left standing for 10 h; crystals filtered and washed with acetone and dried over anhydrous calcium chloride; elem. anal.;

DOI:10.1016/j.poly.2007.04.012

upstream raw materials:

(E)-2-((1,3-diphenyl-1H-pyrazol-4-yl)methylene)hydrazine-1-carbothioamide

nickel(II) acetate tetrahydrate