C₃₇H₄₀N₆

Base Information

• Chemical Name: C₃₇H₄₀N₆
• CAS No.: 1383617-70-6
• Molecular Formula: C₃₇H₄₀N₆
• Molecular Weight: 568.765
• Mol file: 1383617-70-6.mol

Synonyms:

Chemical Property of C₃₇H₄₀N₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₄₀N₆

There total 3 articles about C₃₇H₄₀N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H44N2 (501025-67-8) → C37H40N6 (1383617-70-6)

Guidance literature:

C₃₇H₄₄N₂; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 1h;

With sodium azide; In water; at 4 ℃; for 12h;

DOI:10.1002/cjoc.201100339

Reference yield:

tert-butyl (4-bromophenyl)carbamate (131818-17-2) → C37H40N6 (1383617-70-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / Reflux

2.1: hydrogenchloride / diethyl ether; water / 24 h / 20 °C

3.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

3.2: 12 h / 4 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; sodium nitrite; In tetrahydrofuran; diethyl ether; water; 1.1: Suzuki coupling;

DOI:10.1002/cjoc.201100339

Reference yield:

9,9-dihexyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)fluorene (254755-24-3) → C37H40N6 (1383617-70-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / Reflux

2.1: hydrogenchloride / diethyl ether; water / 24 h / 20 °C

3.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

3.2: 12 h / 4 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; sodium nitrite; In tetrahydrofuran; diethyl ether; water; 1.1: Suzuki coupling;

DOI:10.1002/cjoc.201100339

upstream raw materials:

C₃₇H₄₄N₂

tert-butyl (4-bromophenyl)carbamate

9,9-dihexyl-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)fluorene