4-{[(E)-(3-nitrophenyl)methylidene]amino}benzoic acid

Base Information

• Chemical Name: 4-{[(E)-(3-nitrophenyl)methylidene]amino}benzoic acid
• CAS No.: 3996-28-9
• Molecular Formula: C14H10 N2 O4
• Molecular Weight: 270.2402
• Mol file: 3996-28-9.mol

Synonyms:Benzoicacid, p-[(m-nitrobenzylidene)amino]- (6CI,7CI,8CI); NSC 209038

Chemical Property of 4-{[(E)-(3-nitrophenyl)methylidene]amino}benzoic acid

Chemical Property:

• Vapor Pressure: 1.1E-10mmHg at 25°C
• Boiling Point: 496.7°C at 760 mmHg
• Flash Point: 254.2°C
• Density: 1.31g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-{[(E)-(3-nitrophenyl)methylidene]amino}benzoic acid

There total 2 articles about 4-{[(E)-(3-nitrophenyl)methylidene]amino}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.07%

3-nitro-benzaldehyde (99-61-6) + 4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → N-(3-nitrobenzylidene)-4-aminobenzoic acid (3996-28-9)

Guidance literature:

In ethanol; at 25 ℃; for 24h;

Reference yield:

→ N-(3-nitrobenzylidene)-4-aminobenzoic acid (3996-28-9)

Guidance literature:

4-Carboxy-anilin, 3-Nitro-benzaldehyd;

Reference yield:

nabumetone (42924-53-8) + N-(3-nitrobenzylidene)-4-aminobenzoic acid (3996-28-9) → C29H26N2O6 (1206182-11-7)

Guidance literature:

With hydrogenchloride; In ethanol; chloroform; water; at 25 - 30 ℃;

DOI:10.1007/s11426-012-4816-2

upstream raw materials:

3-nitro-benzaldehyde

4-amino-benzoic acid

Downstream raw materials:

C₂₉H₂₆N₂O₆