carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese

Base Information

Chemical Name:carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese
CAS No.:1357385-34-2
Molecular Formula:C₂₄H₂₀MnNO₂Se₃Sn
Molecular Weight:764.956
Hs Code.:

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Chemical Property of carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese

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Technology Process of carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese

There total 1 articles about carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1666-13-3
diphenyl diselenide

: trichlorostannyl manganese cyclopentadienylcarbonylnitrosyl complex

: 1357385-34-2
carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese

Guidance literature:: With NaBH₄; In ethanol; (Ar), NaBH4 added to a stirred soln. of Ph2Se2 in EtOH, reacted for 1 h,treated with solid Mn complex, stirred for 1 h; evapd.(vac.), extd.(CH2Cl2), chromy.(TLC - CH2Cl2/hexane 2:1), chromy.(silica gel - CH2Cl2), evapd., dissolved (hot hexane), crystd. at room temp. for 2 h, dried, elem. anal.;
DOI:10.1134/S1070328411110108

Reference yield: 52.0%

: 15308-61-9
(diphenylacetylene)bis(triphenylphosphine)platinum⁽⁰⁾

: 1357385-34-2
carbonylcyclopentadienylnitrosyltris(selenophenyl)stannylmanganese

: 52653-84-6,76188-91-5
bis(selenophenyl)bis(triphenylphosphine)platinum(II)

Guidance literature:: In tetrahydrofuran; (Ar), soln. of Pt complex in THF added to a stirred soln. of Mn complex (1:1) in THF, stirred for 1 h; evapd.(vac.), dissolved (Et2O), filtered, diluted (heptane), chromy.(TLC- Et2O/heptane 1:1), kept at -5°C for 24 h, dried (vac.), elem. anal.;
DOI:10.1134/S1070328411110108