C₂₈H₃₅NO₃

Base Information

Chemical Name:C₂₈H₃₅NO₃
CAS No.:104115-53-9
Molecular Formula:C₂₈H₃₅NO₃
Molecular Weight:433.591
Hs Code.:

C<sub>28</sub>H<sub>35</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₅NO₃

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of C₂₈H₃₅NO₃

There total 28 articles about C₂₈H₃₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104115-44-8,1460-38-4
(2-oxocyclopent)acetic acid

: 104115-53-9,104115-59-5
C₂₈H₃₅NO₃

Guidance literature:: Multi-step reaction with 10 steps

1: 89 percent / triethylamine, ethyl chloroformate

2: 83 percent / p-toluenesulfonic acid

3: 73 percent / LDA / tetrahydrofuran

4: 1.) Lawesson's reagent, 2.)ethylene glycol, p-toluenesulfonic acid / 1.) THF 2.) benzene, reflux

5: 84 percent / LDA / tetrahydrofuran / 0 °C

6: 74 percent / triethyloxonium fluoborate, triethylamine / CHCl₃

7: 1.) trimethyloxonium fluoborate; 2.)NaBH₄ / 1.) CH₂Cl₂, 0 deg C; 2.) methanol

9: LDA / tetrahydrofuran / -78 °C

With Lawessons reagent; sodium tetrahydroborate; trimethoxonium tetrafluoroborate; triethyloxonium fluoroborate; chloroformic acid ethyl ester; toluene-4-sulfonic acid; ethylene glycol; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1021/ja00278a061

Reference yield:

: 104115-45-9
N-<2-(2-Methyl-1,3-dioxolan-2-yl)ethyl>-2-oxocyclopentaneacetamide

: 104115-53-9,104115-59-5
C₂₈H₃₅NO₃

Guidance literature:: Multi-step reaction with 9 steps

1: 83 percent / p-toluenesulfonic acid

2: 73 percent / LDA / tetrahydrofuran

3: 1.) Lawesson's reagent, 2.)ethylene glycol, p-toluenesulfonic acid / 1.) THF 2.) benzene, reflux

4: 84 percent / LDA / tetrahydrofuran / 0 °C

5: 74 percent / triethyloxonium fluoborate, triethylamine / CHCl₃

6: 1.) trimethyloxonium fluoborate; 2.)NaBH₄ / 1.) CH₂Cl₂, 0 deg C; 2.) methanol

8: LDA / tetrahydrofuran / -78 °C

With Lawessons reagent; sodium tetrahydroborate; trimethoxonium tetrafluoroborate; triethyloxonium fluoroborate; toluene-4-sulfonic acid; ethylene glycol; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1021/ja00278a061

Reference yield:

: 104115-46-0
C₁₃H₁₉NO₃

: 104115-53-9,104115-59-5
C₂₈H₃₅NO₃

Guidance literature:: Multi-step reaction with 8 steps

1: 73 percent / LDA / tetrahydrofuran

2: 1.) Lawesson's reagent, 2.)ethylene glycol, p-toluenesulfonic acid / 1.) THF 2.) benzene, reflux

3: 84 percent / LDA / tetrahydrofuran / 0 °C

4: 74 percent / triethyloxonium fluoborate, triethylamine / CHCl₃

5: 1.) trimethyloxonium fluoborate; 2.)NaBH₄ / 1.) CH₂Cl₂, 0 deg C; 2.) methanol

7: LDA / tetrahydrofuran / -78 °C

With Lawessons reagent; sodium tetrahydroborate; trimethoxonium tetrafluoroborate; triethyloxonium fluoroborate; toluene-4-sulfonic acid; ethylene glycol; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1021/ja00278a061