Technology Process of C44H30Cl2O4P2Pt
There total 7 articles about C44H30Cl2O4P2Pt which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine
2: triethylamine / diethyl ether; tetrahydrofuran / 20 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
3: dichloromethane; acetonitrile / 16 h / 20 °C / Schlenk technique; Inert atmosphere
With
triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/ejic.201301255
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / -78 °C / Schlenk technique; Inert atmosphere
1.2: 20 h / -78 - 20 °C / Schlenk technique; Inert atmosphere
2.1: boron tribromide; sodium hydrogencarbonate / dichloromethane; water / 20 h / -78 - 20 °C / Schlenk technique; Inert atmosphere
3.1: triethylamine / diethyl ether; tetrahydrofuran / 20 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
4.1: dichloromethane; acetonitrile / 16 h / 20 °C / Schlenk technique; Inert atmosphere
With
tert.-butyl lithium; boron tribromide; sodium hydrogencarbonate; triethylamine;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/ejic.201301255
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(l) chloride / 1-methyl-pyrrolidin-2-one / 120 °C / Schlenk technique; Inert atmosphere
2.1: tert.-butyl lithium / hexane; tetrahydrofuran / 1 h / -78 °C / Schlenk technique; Inert atmosphere
2.2: 20 h / -78 - 20 °C / Schlenk technique; Inert atmosphere
3.1: boron tribromide; sodium hydrogencarbonate / dichloromethane; water / 20 h / -78 - 20 °C / Schlenk technique; Inert atmosphere
4.1: triethylamine / diethyl ether; tetrahydrofuran / 20 h / 0 - 20 °C / Schlenk technique; Inert atmosphere
5.1: dichloromethane; acetonitrile / 16 h / 20 °C / Schlenk technique; Inert atmosphere
With
2,2,6,6-tetramethylheptane-3,5-dione; tert.-butyl lithium; boron tribromide; sodium hydrogencarbonate; caesium carbonate; triethylamine; copper(l) chloride;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/ejic.201301255