N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

Chemical Name:N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside
CAS No.:1443034-35-2
Molecular Formula:C₇₃H₇₄N₂O₂₀
Molecular Weight:1299.39
Hs Code.:

N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Chemical Property of N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 1 articles about N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443018-38-9
C₂₀H₂₄N₂O₆

: 1443034-30-7
C₅₀H₅₁O₁₄P

: 1443034-32-9
C₅₆H₆₂NO₁₅P

: 1443034-35-2
N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Guidance literature:: C₂₀H₂₄N₂O₆; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; at 60 ℃; under 150.015 Torr; Inert atmosphere; Automated synthesizer;

With cesium acetate; In N,N-dimethyl-formamide; at 60 ℃; under 150.015 Torr; Inert atmosphere; Automated synthesizer;

C₅₀H₅₁O₁₄P; C₅₆H₆₂NO₁₅P; Further stages;
DOI:10.1002/anie.201210176

Reference yield:

: 1443034-35-2
N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

: 1443034-36-3
N-benzyloxycarbonyl-5-amino-pentanyl α-D-mannopyranosyl-(1→6)-α-D-mannopyranoside

Guidance literature:: N-benzyloxycarbonyl-5-amino-pentanyl 6-O-(6-aminohexanoyl)-(2,3,4-tri-O-benzoyl-α-D-mannopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside; With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

With sodium methylate; In methanol; water; at 20 ℃; pH=12; Inert atmosphere;
DOI:10.1002/anie.201210176