C₂₃H₂₃F₃N₄O₄

Base Information

Chemical Name:C₂₃H₂₃F₃N₄O₄
CAS No.:1404115-04-3
Molecular Formula:C₂₃H₂₃F₃N₄O₄
Molecular Weight:476.455
Hs Code.:

C<sub>23</sub>H<sub>23</sub>F<sub>3</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₃H₂₃F₃N₄O₄

Chemical Property:

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Technology Process of C₂₃H₂₃F₃N₄O₄

There total 6 articles about C₂₃H₂₃F₃N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60610-72-2
1-(2-Chlor-6-methoxyphenyl)-2-nitroaethylen

: 1404115-04-3
C₂₃H₂₃F₃N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / diethyl ether / 0 °C

2: potassium carbonate; potassium iodide / acetonitrile

3: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / isopropyl alcohol / Heating

4: ammonium formate; 10% Pd/C / methanol / Heating

5: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

With lithium aluminium tetrahydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 10% Pd/C; ammonium formate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; potassium iodide; In methanol; diethyl ether; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile; 3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.031

Reference yield:

: 29866-54-4
2-chloro-6-methoxybenzaldehyde

: 1404115-04-3
C₂₃H₂₃F₃N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1: ammonium acetate / Heating

2: lithium aluminium tetrahydride / diethyl ether / 0 °C

3: potassium carbonate; potassium iodide / acetonitrile

4: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / isopropyl alcohol / Heating

5: ammonium formate; 10% Pd/C / methanol / Heating

6: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

With lithium aluminium tetrahydride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 10% Pd/C; ammonium acetate; ammonium formate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; potassium iodide; In methanol; diethyl ether; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile; 4: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.031

Reference yield:

: C₂₈H₂₉N₃O₂

: 1404115-04-3
C₂₃H₂₃F₃N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate; 10% Pd/C / methanol / Heating

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

With 10% Pd/C; ammonium formate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.08.031