rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO)

Base Information

• Chemical Name: rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO)
• CAS No.: 913171-03-6
• Molecular Formula: C₂₁H₂₆ClFeNOPtS
• Molecular Weight: 626.89
• Mol file: 913171-03-6.mol

Synonyms:

Chemical Property of rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO)

There total 1 articles about rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

cis-dichlorobis(dimethylsulfoxide)platinum(II) (75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9) + 1-[(methyl(phenylmethyl)amino)methyl]ferrocene (227805-06-3) → rac-σPt[(η5-Cp)Fe(η5-C5H3-CH2N(methyl)-benzyl)](chloride)(DMSO) (913171-03-6)

Guidance literature:

In methanol; (N2); to a stirred soln. of amine in methanol cis-Pt(DMSO)2Cl2 added; mixture stirred and refluxed for 30 min; cooled back to room temp.; solvent removed in vacuo; water added; extracted with CH2Cl2 and separated; organic layer dried over anhydrous Na2SO4 and filtered; chromy. (silica gel, ethyl acetate/hexane=1:5 v/v); elem. anal.;

DOI:10.1016/j.poly.2006.02.017

upstream raw materials:

cis-dichlorobis(dimethylsulfoxide)platinum(II)

1-[(methyl(phenylmethyl)amino)methyl]ferrocene