Technology Process of C36H37BN2O5
There total 3 articles about C36H37BN2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H20N2O3;
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
2-(4-(iodomethyl)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja308124q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate; C16H36N; tris-(o-tolyl)phosphine; palladium diacetate / N,N-dimethyl-formamide / 100 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
With
palladium diacetate; potassium carbonate; C16H36N; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
DOI:10.1021/ja308124q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate; C16H36N; tris-(o-tolyl)phosphine; palladium diacetate / N,N-dimethyl-formamide / 100 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
With
palladium diacetate; potassium carbonate; C16H36N; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
DOI:10.1021/ja308124q
