(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

Base Information

Chemical Name:(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate
CAS No.:1365543-89-0
Molecular Formula:C₂HF₃O₂*C₄₆H₄₈N₁₄O₄
Molecular Weight:975.002
Hs Code.:

(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

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Chemical Property of (R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

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Technology Process of (R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

There total 8 articles about (R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 4-[methyl(prop-2-ynyl)amino]pyridinium chloride

: (R)-1-(1-(4-Azidophenyl)-1H-1,2,3-triazol-4-yl)-10-(4-hydroxybenzylcarbamoyl)-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecan-5-iminium 2,2,2-trifluoroacetate

: 76-05-1
trifluoroacetic acid

: 1365543-89-0
(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

Guidance literature:: 4-[methyl(prop-2-ynyl)amino]pyridinium chloride; (R)-1-(1-(4-Azidophenyl)-1H-1,2,3-triazol-4-yl)-10-(4-hydroxybenzylcarbamoyl)-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecan-5-iminium 2,2,2-trifluoroacetate; With copper(ll) sulfate pentahydrate; C₃₀H₂₄N₁₀O₆; ascorbic acid; In methanol; water; dimethyl sulfoxide; at 65 ℃; for 1h; Alkaline aq. solution;

trifluoroacetic acid; In methanol; water; dimethyl sulfoxide;
DOI:10.1135/cccc2011036

Reference yield:

: 1365610-18-9
4-(N-methyl-N-propargylamino)pyridine

: 1365543-89-0
(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / pH 0 - 2

2: copper(ll) sulfate pentahydrate; C₃₀H₂₄N₁₀O₆; ascorbic acid / methanol; water; dimethyl sulfoxide / 1 h / 65 °C / Alkaline aq. solution

With hydrogenchloride; copper(ll) sulfate pentahydrate; C₃₀H₂₄N₁₀O₆; ascorbic acid; In methanol; water; dimethyl sulfoxide;
DOI:10.1135/cccc2011036

Reference yield:

: 1365544-00-8
tert-butyl [(1-(4-azidophenyl)-1H-1,2,3-triazol-4-yl)methyl]carbamate

: 1365543-89-0
(R)-4-(((1-(4-(4-(10-(4-hydroxybenzylcarbamoyl)-5-imino-3,12-dioxo-13,13-diphenyl-2,4,6,11-tetraazatridecyl)-1H-1,2,3-triazol-1-yl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-(methyl)amino)pyridinium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 1 h

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

2.2: 20 °C

3.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide

3.2: 2 h

4.1: copper(ll) sulfate pentahydrate; C₃₀H₂₄N₁₀O₆; ascorbic acid / methanol; water; dimethyl sulfoxide / 1 h / 65 °C / Alkaline aq. solution

With copper(ll) sulfate pentahydrate; C₃₀H₂₄N₁₀O₆; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride; ascorbic acid; In methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1135/cccc2011036