Technology Process of C34H28F6O5(18)O
There total 3 articles about C34H28F6O5(18)O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Daicel Chiralpak IA / hexane; isopropyl alcohol / Resolution of racemate; Inert atmosphere
2: 2-methoxy-ethanol; sodium; 18O-labeled water / 95 °C / Inert atmosphere
3: dmap / pyridine / 18 h / 20 °C / Inert atmosphere
With
dmap; 2-methoxy-ethanol; sodium; 18O-labeled water;
In
pyridine; hexane; isopropyl alcohol;
DOI:10.1002/anie.201102263
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; Diphenylphosphinic chloride / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: 2-methoxy-ethanol; sodium; 18O-labeled water / 95 °C / Inert atmosphere
3.1: dmap / pyridine / 18 h / 20 °C / Inert atmosphere
With
pyridine; dmap; 2-methoxy-ethanol; sodium; 18O-labeled water; Diphenylphosphinic chloride;
In
pyridine;
DOI:10.1002/anie.201102263
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2-methoxy-ethanol; sodium; 18O-labeled water / 95 °C / Inert atmosphere
2: dmap / pyridine / 18 h / 20 °C / Inert atmosphere
With
dmap; 2-methoxy-ethanol; sodium; 18O-labeled water;
In
pyridine;
DOI:10.1002/anie.201102263