[(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl

Base Information

Chemical Name:[(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl
CAS No.:1253202-07-1
Molecular Formula:C₁₄H₁₉Cl₂N₂PdS₂*Cl
Molecular Weight:492.229
Hs Code.:

[(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl<sub>2</sub>]Cl

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Chemical Property of [(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl

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Technology Process of [(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl

There total 1 articles about [(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 1253202-04-8
N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium chloride

: 1253202-07-1
[(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl

Guidance literature:: In dichloromethane; (inert atmosphere); Pd complex added to a soln. of ligand, stirred for 4h; volatiles removed via cannula, washed (pentane), dried (vac.); elem. anal.;
DOI:10.1039/c0dt00351d

Reference yield: 74.0%

: 17084-13-8
potassium hexafluorophosphate

: 1253202-07-1
[(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazolium)PdCl₂]Cl

: [(N-ethyl-methyl-sulfide-N'-ethyl-phenyl-sulfide imidazol-2-ylidene)PdCl]PF₆

Guidance literature:: With Cs₂CO₃; In acetonitrile; (inert atmosphere); Cs2CO3 added to a suspn. of Pd complex and KPF6, refluxed for 6 h; filtered, evapd. (vac.), washed (pentane); elem. anal.;
DOI:10.1039/c0dt00351d