C₂₀H₃₀O₄

Base Information

Chemical Name:C₂₀H₃₀O₄
CAS No.:1354575-85-1
Molecular Formula:C₂₀H₃₀O₄
Molecular Weight:334.456
Hs Code.:

C<sub>20</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₃₀O₄

Chemical Property:

Purity/Quality:

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Technology Process of C₂₀H₃₀O₄

There total 15 articles about C₂₀H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354575-84-0
C₂₀H₂₉IO₄

: 1354575-85-1
C₂₀H₃₀O₄

Guidance literature:: C₂₀H₂₉IO₄; With sodium iodide; zinc; In methanol; at 90 ℃; for 2.5h; Inert atmosphere;

With water; In methanol; Inert atmosphere;
DOI:10.1038/ja.2011.90

Reference yield:

: C₁₈H₃₆O₃Si

: 1354575-85-1
C₂₀H₃₀O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 20 °C / Inert atmosphere

2.1: trimethylamine hydrochloride; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: sodium iodide / acetone / 8.5 h / Inert atmosphere; Reflux

4.1: tert.-butyl lithium / diethyl ether; pentane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

4.3: 0 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: pyridinium p-toluenesulfonate / methanol / 5 h / 20 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / 18 h / -20 °C / Molecular sieve; Inert atmosphere

7.2: -20 °C / Inert atmosphere

8.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran; acetonitrile / 0 - 20 °C / Inert atmosphere

9.1: sodium iodide; zinc / methanol / 2.5 h / 90 °C / Inert atmosphere

9.2: Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; tetrapropylammonium perruthennate; diethyl (2S,3S)-tartrate; tetrabutyl ammonium fluoride; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; trimethylamine hydrochloride; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; sodium iodide; zinc; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone; acetonitrile; pentane; 7.1: Sharpless asymmetric epoxidation;
DOI:10.1038/ja.2011.90

Reference yield:

: 1354575-73-7
C₁₃H₂₄O₅S

: 1354575-85-1
C₂₀H₃₀O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium iodide / acetone / 8.5 h / Inert atmosphere; Reflux

2.1: tert.-butyl lithium / diethyl ether; pentane / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - 0 °C / Inert atmosphere

2.3: 0 °C / Inert atmosphere

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: pyridinium p-toluenesulfonate / methanol / 5 h / 20 °C / Inert atmosphere

5.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / 18 h / -20 °C / Molecular sieve; Inert atmosphere

5.2: -20 °C / Inert atmosphere

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran; acetonitrile / 0 - 20 °C / Inert atmosphere

7.1: sodium iodide; zinc / methanol / 2.5 h / 90 °C / Inert atmosphere

7.2: Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; tetrapropylammonium perruthennate; diethyl (2S,3S)-tartrate; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triphenylphosphine; sodium iodide; zinc; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone; acetonitrile; pentane; 5.1: Sharpless asymmetric epoxidation;
DOI:10.1038/ja.2011.90