C₃₁H₂₂N₂O₆S₂

Base Information

Chemical Name:C₃₁H₂₂N₂O₆S₂
CAS No.:1374583-97-7
Molecular Formula:C₃₁H₂₂N₂O₆S₂
Molecular Weight:582.657
Hs Code.:

C<sub>31</sub>H<sub>22</sub>N<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₁H₂₂N₂O₆S₂

Chemical Property:

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Technology Process of C₃₁H₂₂N₂O₆S₂

There total 8 articles about C₃₁H₂₂N₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374583-69-3
C₃₃H₂₈N₂O₁₀S₃

: 1374584-03-8
C₃₁H₂₂N₂O₆S₂

: 1374583-97-7
C₃₁H₂₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 4 steps

1: lithium bromide / tetrahydrofuran / 2 h

2: sodium sulfide; tetrabutylammomium bromide / tetrahydrofuran; water / 0 - 20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

4: triethylamine

With sodium sulfide; tetrabutylammomium bromide; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/asia.201100903

Reference yield:

: 2-{3-[2-(3-bromoprop-1-ynyl)phenyl]prop-2-ynyloxy}tetrahydropyran

: 1374584-03-8
C₃₁H₂₂N₂O₆S₂

: 1374583-97-7
C₃₁H₂₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: pyridinium p-toluenesulfonate / ethanol / 50 °C

3: triethylamine / dichloromethane / 0 °C / Inert atmosphere

4: lithium bromide / tetrahydrofuran / 2 h

5: sodium sulfide; tetrabutylammomium bromide / tetrahydrofuran; water / 0 - 20 °C

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

7: triethylamine

With sodium sulfide; tetrabutylammomium bromide; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/asia.201100903

Reference yield:

: 1374583-56-8
C₄₁H₄₀N₂O₈S

: 1374584-03-8
C₃₁H₂₂N₂O₆S₂

: 1374583-97-7
C₃₁H₂₂N₂O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1: pyridinium p-toluenesulfonate / ethanol / 50 °C

2: triethylamine / dichloromethane / 0 °C / Inert atmosphere

3: lithium bromide / tetrahydrofuran / 2 h

4: sodium sulfide; tetrabutylammomium bromide / tetrahydrofuran; water / 0 - 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

6: triethylamine

With sodium sulfide; tetrabutylammomium bromide; pyridinium p-toluenesulfonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/asia.201100903