(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

Base Information

Chemical Name:(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl
CAS No.:1351623-48-7
Molecular Formula:C₃₂H₄₆ClIrN₂O₂P₂
Molecular Weight:780.35
Hs Code.:

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Chemical Property of (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

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Technology Process of (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

There total 1 articles about (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1351623-47-6
2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine

: [(cis-cyclooctene)2IrCl]2

: 1351623-48-7
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

Guidance literature:: With C₂H₄; In diethyl ether; (Ar); soln. of iridium complex was stirred under 1 atm. of C2H4 at -40°C, soln. of pyrazine in Et2O was added. warmed to ambient temp.; evapd. in vac., extd. with toluene, filtered, evapd., washed with cold pentane, elem. anal.;
DOI:10.1039/c1nj20602h

Reference yield: 49.0%

: 1351623-48-7
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

: 2999-74-8
dimethylmagnesium

: 1351623-50-1
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

Guidance literature:: In tetrahydrofuran; toluene; (Ar); mixt. of THF/toluene (0.1:4, v/v) was added to mixt. of iridium complex with Me2Mg, heated to 130°C for 3 d; evapd. in vac., extd. with toluene, concd., crystd. with pentane at -35°C, elem. anal.;
DOI:10.1039/c1nj20602h