catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo

Base Information

Chemical Name:catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo
CAS No.:165965-91-3
Molecular Formula:C₆H₆O₂*C₁₉H₂₂BNO₃
Molecular Weight:433.312
Hs Code.:

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Chemical Property of catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo

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Technology Process of catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo

There total 2 articles about catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.8%

: 160758-66-7
[2-(diisopropylamino)carbonyl]phenylboronic acid

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 165965-91-3
catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo

Guidance literature:: In benzene; byproducts: water; N2-atmosphere; azeotropic distn. off of water from soln. of boronic acid, addn. of catechol at 70°C, distn. off of water for 3 h; evapn.; can be recrystallized (PhMe); elem. anal.;
DOI:10.1016/0022-328X(94)05337-B

Reference yield:

: 20383-28-2
N,N-diisopropyl benzamide

: 165965-91-3
catechol [2-(diisopropylamino)carbonyl]phenylboronate * catechlo

Guidance literature:: Multi-step reaction with 2 steps

1: TMEDA; sec-BuLi / tetrahydrofuran

2: benzene

With TMEDA; sec-BuLi; In tetrahydrofuran; benzene;
DOI:10.1016/0022-328X(94)05337-B